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Specific expertise includes Handling air-sensitive compounds - 50mL to 500gal scale - Schlenk-line/Vacuum; Glove-Box - Cogeim and Neutsch filters Instruments - NMR (300 and 400 MHz) - In-situ FT-IR - GC, GCMS, HPLC, UV-VIS, AA - Wiped-Film Evaporator - SEM Reactions at commercial scale - Grignard and alkyl lithium reagents - Friedal-Crafts alkylation - Acid-catalyzed dehydration - Ligand metallation (Ti, Zr, Hf) - Amination/Condensation - Organosilane - Borohydride reduction - Catalytic cross-coupling - Suzuki-type coupling - Kinetics - Strong bases (alkoxides, metal hydrides) - Thermal cracking - Hydrogenation - Alkoxylations - Amination - Carboxylation |